X-ray 3D Microscope TriLambdaXRM-30

Key Advantages:

Nanoscale 35nm Spatial Resolution

The TriLambda nanoXRM achieves over an order of magnitude in superior resolution compared to lensless x-ray microscopes such as the PrismaXRM, which do not use x-ray optics. Such resolution is achieved through the use of Sigray’s proprietary double paraboloidal x-ray optics and diffractive focusing zone plate optics. PrismaXRM and TriLambdaXRM provide natural multi-scale complements to each other; PrismaXRM provides submicron imaging of larger samples, while the TriLambda provides 35-100nm resolution imaging of smaller samples.

Outstanding 35-50nm resolutions can be achieved for x-ray energies ranging from 2.7 keV to 8.04 keV.

Three X-ray Wavelengths (Tri-Lamba) in a Single System

Up to three x-ray energies are included in the TriLambda system, providing optimal illumination for the wide range of samples seen in a busy central laboratory. X-ray contrast varies significantly for each x-ray energy, impacting both the time to acquire data and more importantly, the visibility of structures. For example, 5.4 keV is optimal for geological samples (SiO2) but poor for samples with metal in them. For polymers and cells, soft x-ray energies (2.7 keV) provide profound advantages over 8 keV.

Dual Energy (Dual Contrast)

Interpreting contrast measurements and CT numbers can be a difficult task when only a single X-ray energy is used for imaging. This is due to the presence of sub-resolution features, such as nanoporosity or nano-scale alloying elements that change the absorption of a sample and lead to errors in image segmentation and inaccurate quantification of the atomic number of a material. By imaging at two different x-ray illumination energies (dual energy), TriLambda removes such errors.

3D surface rendering of segmented Fe NPs (orange) in relation to the graphite clusters acquired with dual contrast

 

 

Batteries

The microstructure of electrodes are increasingly of interest because it is now recognized that damage incurred and agglomeration of particles from charging limits the long-term reliability and lifetime. TriLambdaXRM provides the resolution needed to see these changes – and because of the non-destructive nature of x-rays, can be used to observe such changes over time or in-operando.

Polymers and Biological Samples

A key feature of the TriLambdaXRM is its ability to resolve polymers and biological samples at the nanoscale. Such samples are extremely challenging to image using electron-based techniques due to charging. Using a low “tender” x-ray energy to illuminate the sample at 2.7 keV, TriLambda is able to provide 3D nanoscale biological and polymeric tomographies non-destructively.

 

Technical Specifications of the TriLambda-30

 ParameterSpecification
OverallSpatial ResolutionMinimum 35nm spatial resolution at 2,7 keV
SourceType(s)Patented multi-target reflection source
Voltage20-50 kVp
Target(s)Up to 3 targets.
Si, Cr, Fe, Cu
ModesResolution and FOV Settings3 high resolution modes and 1 LFOV mode
LFOV Mode120nm resolution | 65nm voxel
65 μm FOV | 60 μm diameter optimal
OpticsCondensers3 sets of Sigray Double Paraboloidal x-ray optics matched to zone plates
Focusing ObjectiveFresnel diffraction zone plates
Phase RingZernike phase shift ring
SoftwareCommand and ControlSigray 3D with Intuitive interface
ReconstructionGigaRecon - fastest commercial CBCT reconstruction software
Linux WorkstationInterface is on a Windows workstation, while a separate robust Linux workstation controls the system. Advantageous for reliable 24-7 operation.
EPICSOpen-source software controls for maximum flexibility
DimensionsFootprint2.3m L x 1.3m W x 1.5m H

Applications in battery research

https://sigray-site-videos.s3.us-west-1.amazonaws.com/NREL-Cathode-8keV.mp4

Application in polymer research and biological samples

https://sigray.com/assets/Fruit-fly-brain.m4v

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