Large geometry MC-ICP-MS NU Plasma 1700

Introduction The application of non-traditional stable isotope systems such as Mg, Si, S, K, Ca, Ti, V, Cr, Fe, Ni and Se in geochemistry, cosmochemistry and life sciences has been spurred by the advancement of the multi-collector ICP-MS (MC-ICPMS) over the last two decades. This versatile technique, although widely considered as the standard method for the high precision isotopic analysis of such systems, is limited by the inevitable molecular species generated by the ICP source resulting from ions such as Ar+, N+, O+ and H+. These species can often interfere directly with the atomic ions of the same nominal mass, leading to inaccurate isotope ratio determination. The ability to avoid unwanted interfering species in close proximity to the target ions on the mass focal plane is dependent on the mass resolution. Such interfering species are partially resolved by narrowing the source entrance slit to proportionally increase the mass resolution.

Nu Plasma 1700 is a unique High Resolution Multi Collector ICP-MS from Nu Instruments providing the ultimate in high resolution isotope ratio measurements. The instrument has been designed with a high dispersion and large geometry to provide a no compromise high resolution capability whilst still maintaining flat top peaks for high precision measurements with minimal loss in sensitivity.

Peak flat at 5,000 resolution 

The Nu Plasma 1700’s large geometry uniquely allows resolutions of >5,000 while maintaining peak flat. Each of its sixteen Faraday detectors and five full size discrete dynode multipliers have independent variable high-resolution slits allowing different resolutions on individual detectors. When the highest performing MC-ICP-MS is required, the Nu Plasma 1700 is the no compromise solution.

Sapphire 1700 combines the Plasma 1700 mass analyser with the dual transfer optics from the Sapphire, including a “high energy” ion path (traditional MC-ICP-MS) and a separate “low energy” ion path (collision/reaction cell), offering the benefits of collision/reaction cell without compromising performance on classical geological applications. The ‘dual path’ design allows the cell to be used to remove isobaric interferences for special applications, and fully bypassed when analyzing classical isotope systems that do not require removal of interferences.

  • Double-focussing high-resolution MC-ICP-MS with large dispersion
  • Enhanced Sensitivity Interface as standard.
  • Moveable Faraday detectors on the outer array providing extra flexibility for large dispersion isotope systems
  • Better abundance sensitivity than a standard MC-ICP-MS
  • True high resolution and pseudo high resolution analysis capability
  • Variable independently adjustable high resolution collector slit for each collector
  • Sixteen large dynamic range Faraday detectors, with optional software switchable resistor pre-amplifiers
  • Up to five ion-counting detectors (with SEM/Daly options) and high abundance deceleration filters for improved abundance sensitivity Standard resolution >800, Peak flat at >5000 resolution
  • Differential pumping configuration
  • Ground potential analyser operation
  • Variable Zoom Optics allow for instantaneous switching between isotopic systems during analysis
  • Fully Dry Pumped configuration available

The Plasma 1700 has a unique true high resolution capability, utilizing independently adjustable collector slits fitted for each detector. Interfering peaks are completely resolved from analyte peaks, whilst maintaining a flat top profile. This is critical in cases when polyatomic interferences appear on the high mass side and doubly charged interferences on the low mass side of the analyte peaks, often observed in laser ablation mode. 

As a result of its higher transmission, sample-standard bracketing results of repeat measurements of a 100ppb Si standard solution and a 150ppb Fe standard solution yield precisions typically achieved on a standard MC-ICP-MS using solutions several times more concentrated. Plasma 1700 is thus particularly advantageous for isotopic analysis of samples of limited size.

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